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Registros recuperados : 14 | |
1. | | GARCIA, R. H. S.; COLNAGO, L. A. Desenvolvimento de sequência de pulso em RMN-DT para caracterização de sementes de soja In: JORNADA CIENTÍFICA - EMBRAPA SÃO CARLOS, 8., 2016, São Carlos, SP. Anais... São Carlos: Embrapa Instrumentação: Embrapa Pecuária Sudeste, 2016. p.89. Editores técnicos: Wilson Tadeu Lopes da Silva, José Manoel Marconcini, Maria Alice Martins, Lucimara Aparecida Forato, Paulino Ribeiro Villas Boas. (Embrapa Instrumentação. Documentos, 61). Biblioteca(s): Embrapa Instrumentação. |
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2. | | GARCIA, R. H. S.; COLNAGO, L. A. Utilização da RMN-DT no controle de qualidade de manteigas e margarinas. In: SIMPÓSIO NACIONAL DE INSTRUMENTAÇÃO AGROPECUÁRIA, 4., 2019, São Carlos, SP. Ciência, inovação e mercado: anais. São Carlos, SP: Embrapa Instrumentação, 2019. Editores: Paulino Ribeiro Villas-Boas, Maria Alice Martins, Débora Marcondes Bastos Pereira Milori, Ladislau Martin Neto. SIAGRO 2019. 685-689 Biblioteca(s): Embrapa Instrumentação. |
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3. | | GARCIA, R. H. S.; COLNAGO, L. A.; TANNÚS, A. Desenvolvimento e aplicação de pulsos formatados para RMN-DT. In: SIMPÓSIO NACIONAL DE INSTRUMENTAÇÃO AGROPECUÁRIA, 2014, São Carlos, SP Anais do SIAGRO: ciência, inovação e mercado 2014. São Carlos, SP: Embrapa Instrumentação, 2014. p. 245-248. Editores: Carlos Manoel Pedro Vaz, Débora Marcondes Bastos Pereira Milori, Silvio Crestana. Biblioteca(s): Embrapa Instrumentação. |
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8. | | SOUZA, D. G.; RESENDE, O.; PILON, L.; COLNAGO, L. A.; GARCIA, R. H. S.; ALMEIDA, A. B. Functional characterization of biofortified sweet potato flour dried at different temperatures. International Journal for Innovation Education and Research, v. 8, n.12, p. 167-182, 2020. Biblioteca(s): Embrapa Hortaliças; Embrapa Instrumentação. |
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10. | | FACCHINATTO, W. M.; GARCIA, R. H. S.; SANTOS, D. M.; FIAMINGO, A.; FLORES, D. W. M.; CAMPANA-FILHO, S. P.; AZEVEDO, E. R.; COLNAGO, L. A. Fast-forward approach of time-domain NMR relaxometry for solid-state chemistry of chitosan. Carbohydrate Polymers, v. 256, 117576, 2021. 1 - 10 Biblioteca(s): Embrapa Instrumentação. |
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11. | | BIANQUINI, T. S.; FLORENCIO, C.; GARCIA, R. H. S.; COLNAGO, L. A.; CECCATO-ANTONINI, S. R.; CARMO, M.; TELES, J.; FARINAS, C. S.; RIBEIRO, T. S. Time domain NMR spectroscopy as a fast method for probing the efficiency of biomass pretreatments for second generation ethanol production. Biomass and Bioenergy, v. 142, a. 105734, 2020. Biblioteca(s): Embrapa Instrumentação. |
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12. | | MACHADO, G. O.; TEIXEIRA, G. G.; GARCIA, R. H. S.; MORAES, T. B.; BONA, E.; SANTOS, P. M.; COLNAGO, L. A. Non-invasive method to predict the composition of requeijão cremoso directly in commercial packages using time domain NMR relaxometry and chemometrics. Molecules, v. 27, a4434, 2022. 10 p. Biblioteca(s): Embrapa Instrumentação. |
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13. | | SANTOS, Y. J. S.; CAMPOS, N. A.; BICCA, G. B.; SORA, G. T. S.; POLESI, L. F.; ALBERTE, T. M.; SANTOS, P. M.; GARCIA, R. H. S.; COLNAGO, L. A.; OLIVEIRA-FOLADOR. G. Non-destructive determination of the oil content in peach palm (Bactris gasipaes) flour using NMR and NIR spectroscopies. Food Science and Technology, v. 43, e112322, 2023. 1 - 8 Biblioteca(s): Embrapa Instrumentação. |
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14. | | SALVADOR, M. V.; KOCK, F. V. C.; SANTOS, I. L.; PAULINO, J. F. C.; ALMEIDA, C. P. de; GARCIA, R. H. S.; BENCHIMOL-REIS, L. L.; COLNAGO, L. A.; FERREIRA, A. G. Monitoring stimulated darkening from UV-C light on different bean genotypes by NMR spectroscopy. Molecules, v. 27, 2060, 2022. 10 p. Biblioteca(s): Embrapa Instrumentação. |
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Registros recuperados : 14 | |
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Registro Completo
Biblioteca(s): |
Embrapa Instrumentação. |
Data corrente: |
27/04/2022 |
Data da última atualização: |
23/01/2024 |
Tipo da produção científica: |
Artigo em Periódico Indexado |
Circulação/Nível: |
A - 2 |
Autoria: |
SALVADOR, M. V.; KOCK, F. V. C.; SANTOS, I. L.; PAULINO, J. F. C.; ALMEIDA, C. P. de; GARCIA, R. H. S.; BENCHIMOL-REIS, L. L.; COLNAGO, L. A.; FERREIRA, A. G. |
Afiliação: |
LUIZ ALBERTO COLNAGO, CNPDIA. |
Título: |
Monitoring stimulated darkening from UV-C light on different bean genotypes by NMR spectroscopy. |
Ano de publicação: |
2022 |
Fonte/Imprenta: |
Molecules, v. 27, 2060, 2022. |
Páginas: |
10 p. |
DOI: |
https://doi.org/10.3390/molecules27072060 |
Idioma: |
Inglês |
Conteúdo: |
The use of UV-C cool white light on bean (Phaseolus vulgaris L.) seeds significantly increases the biochemical seed coat post-harvest darkening process, whilst preserving seed germination. The aim of this work consists in monitoring the effect caused by the incidence of UV-C light on different bean genotypes using NMR spectroscopy. The genotype samples named IAC Alvorada; TAA Dama;BRS Estilo and BRS Pérola from the Agronomic Institute (IAC; Campinas; SP; Brazil) were evaluated.The following two methodologies were used: a prolonged darkening, in which the grain is placed in a room at a controlled temperature (298 K) and humidity for 90 days, simulating the supermarket shelf; an accelerated darkening, where the grains are exposed to UV-C light (254 nm) for 96 h. The experiments were performed using the following innovative time-domain (TD) NMR approaches:the RK-ROSE pulse sequence; one- and two-dimensional high resolution (HR) NMR experiments(1H; 1H-1H COSY and 1H-13C HSQC); chemometrics tools, such as PLS-DA and heat plots. The results suggest that the observed darkening occurs on the tegument after prolonged (90 days) and accelerated (96 h) conditions. In addition, the results indicate that phenylalanine is the relevant metabolite within this context, being able to participate in the chemical reactions accounted for by the darkening processes. Additionally, it is possible to confirm that a UV-C lamp accelerates oxidative enzymatic reactions and that the NMR methods used were a trustworthy approach to monitor and understand the darkening in bean seeds at metabolite level. MenosThe use of UV-C cool white light on bean (Phaseolus vulgaris L.) seeds significantly increases the biochemical seed coat post-harvest darkening process, whilst preserving seed germination. The aim of this work consists in monitoring the effect caused by the incidence of UV-C light on different bean genotypes using NMR spectroscopy. The genotype samples named IAC Alvorada; TAA Dama;BRS Estilo and BRS Pérola from the Agronomic Institute (IAC; Campinas; SP; Brazil) were evaluated.The following two methodologies were used: a prolonged darkening, in which the grain is placed in a room at a controlled temperature (298 K) and humidity for 90 days, simulating the supermarket shelf; an accelerated darkening, where the grains are exposed to UV-C light (254 nm) for 96 h. The experiments were performed using the following innovative time-domain (TD) NMR approaches:the RK-ROSE pulse sequence; one- and two-dimensional high resolution (HR) NMR experiments(1H; 1H-1H COSY and 1H-13C HSQC); chemometrics tools, such as PLS-DA and heat plots. The results suggest that the observed darkening occurs on the tegument after prolonged (90 days) and accelerated (96 h) conditions. In addition, the results indicate that phenylalanine is the relevant metabolite within this context, being able to participate in the chemical reactions accounted for by the darkening processes. Additionally, it is possible to confirm that a UV-C lamp accelerates oxidative enzymatic reactions and that the NMR methods used were... Mostrar Tudo |
Palavras-Chave: |
Bean darkening; NMR spectroscopy and chemometrics; UV-C irradiation. |
Categoria do assunto: |
-- |
URL: |
https://ainfo.cnptia.embrapa.br/digital/bitstream/doc/1142447/1/P-Monitoring-Stimulated-Darkening-from-UV-C-Light-on.pdf
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Marc: |
LEADER 02434naa a2200277 a 4500 001 2142447 005 2024-01-23 008 2022 bl uuuu u00u1 u #d 024 7 $ahttps://doi.org/10.3390/molecules27072060$2DOI 100 1 $aSALVADOR, M. V. 245 $aMonitoring stimulated darkening from UV-C light on different bean genotypes by NMR spectroscopy.$h[electronic resource] 260 $c2022 300 $a10 p. 520 $aThe use of UV-C cool white light on bean (Phaseolus vulgaris L.) seeds significantly increases the biochemical seed coat post-harvest darkening process, whilst preserving seed germination. The aim of this work consists in monitoring the effect caused by the incidence of UV-C light on different bean genotypes using NMR spectroscopy. The genotype samples named IAC Alvorada; TAA Dama;BRS Estilo and BRS Pérola from the Agronomic Institute (IAC; Campinas; SP; Brazil) were evaluated.The following two methodologies were used: a prolonged darkening, in which the grain is placed in a room at a controlled temperature (298 K) and humidity for 90 days, simulating the supermarket shelf; an accelerated darkening, where the grains are exposed to UV-C light (254 nm) for 96 h. The experiments were performed using the following innovative time-domain (TD) NMR approaches:the RK-ROSE pulse sequence; one- and two-dimensional high resolution (HR) NMR experiments(1H; 1H-1H COSY and 1H-13C HSQC); chemometrics tools, such as PLS-DA and heat plots. The results suggest that the observed darkening occurs on the tegument after prolonged (90 days) and accelerated (96 h) conditions. In addition, the results indicate that phenylalanine is the relevant metabolite within this context, being able to participate in the chemical reactions accounted for by the darkening processes. Additionally, it is possible to confirm that a UV-C lamp accelerates oxidative enzymatic reactions and that the NMR methods used were a trustworthy approach to monitor and understand the darkening in bean seeds at metabolite level. 653 $aBean darkening 653 $aNMR spectroscopy and chemometrics 653 $aUV-C irradiation 700 1 $aKOCK, F. V. C. 700 1 $aSANTOS, I. L. 700 1 $aPAULINO, J. F. C. 700 1 $aALMEIDA, C. P. de 700 1 $aGARCIA, R. H. S. 700 1 $aBENCHIMOL-REIS, L. L. 700 1 $aCOLNAGO, L. A. 700 1 $aFERREIRA, A. G. 773 $tMolecules$gv. 27, 2060, 2022.
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